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2023年1月1日 · The GC column was initially heated at 40 °C, the temperature was then increased at 3.8 °C/min to 200 °C, then raised by 30 °C/min to 240 °C and kept constant for the final 15 min. The carrier gas was helium at a flow rate of 1.2 mL/min. EI mode (70 eV) was used to acquire mass spectra in the 30–350 m / z range.

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