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2017/03/15 · Sci. 15 (1977) 196 – 197]. Procedure: Dissolve 0.1 to 1 mg of the sample in 0.1 ml solvent, add 0.1 ml HFBA and heat to 60 – 70 °C for 1 – 2 hours. If the sample need not be concentrated prior to the analysis and if there is no danger of catalytically induced side reactions, pyridine is used as solvent.

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